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Current Instrumental Methods of Inorganic Substances Analysis
Спеціальність: Chemistry
Код дисципліни: 8.102.00.M.25
Кількість кредитів: 3
Кафедра: Physical, Analytical and General Chemistry
Лектор: Associate Professor, Ph.D. Polyuzhyn I.P.
Семестр: 4 семестр
Форма навчання: денна
Результати навчання:
- knowledge of the phenomena underlying certain instrumental methods of analyzing the chemical composition of inorganic substances;
- knowledge of the laws that relate the structure of a compound and its number to certain parameters of the analytical signal;
- ability to apply knowledge of the theory and practice of modern instrumental methods of analysis to solving real-world problems of determining the chemical composition of inorganic substances, as well as the choice of optimal conditions for sample preparation and obtaining analytical signal.
- knowledge of the laws that relate the structure of a compound and its number to certain parameters of the analytical signal;
- ability to apply knowledge of the theory and practice of modern instrumental methods of analysis to solving real-world problems of determining the chemical composition of inorganic substances, as well as the choice of optimal conditions for sample preparation and obtaining analytical signal.
Необхідні обов'язкові попередні та супутні навчальні дисципліни:
Modern Organic Chemistry
Chemical thermodynamics
Modern methods of identification of organic compounds
Heterogeneous catalysis
Solution theories and phase equilibrium for graduate students
Chemical thermodynamics
Modern methods of identification of organic compounds
Heterogeneous catalysis
Solution theories and phase equilibrium for graduate students
Короткий зміст навчальної програми:
Possibilities of modern instrumental methods of analysis for the investigation of the chemical composition of inorganic substances. Presentation of the results of the chemical composition analysis. Uncertainty of measurement. Sample preparation is the first stage of the analytical process. X-ray fluorescence analysis. X-ray-structural analysis. Thermogravimetry. Atomic emission spectral analysis. Atomic absorption spectral analysis. Molecular absorption spectroscopy in the infrared region for the study of inorganic substances. Molecular absorption spectroscopy in visible and ultraviolet regions for the study of inorganic substances. Electron paramagnetic resonance. Electrochemical methods of analysis and their classification according to IUPAC. Conductometric methods of analysis. Potentiometric methods of analysis. Voltamperometric methods of analysis. Mass spectrometry of inorganic substances. Ion exchange chromatography for the separation and determination of cations and anions in aqueous solutions.
Рекомендована література:
1. Analitychna khimiya. Problemy ta pidkhody. T. 1, 2 / Pod red. YU. A. Zolotova. - M.: Svit, AST, 2004. - T. 1. - 608 s., T. 2. - 728 s.
2. Minayeva V. O. Khromatohrafichniy analiz. - Cherkasy: Vyd. vid. CHNU imeni Bohdana Khmel?nyts?koho, 2013. - 284 s.
3. Minaeva V.O. Metody kontsentruvannya neorhanichnikh Rechovyny / V.O. Minaeva. Navch-met. posibnyk. - Cherkasy: Vyd. vid. CHNU imeni Bohdana Khmel?nyts?koho, 2014. - 313 s.
4. Otto M. Suchasni metody analitychnoyi khimiyi (v 2-kh tomakh) Tom 2. Moskva: Tekhnosfera, 2004. – 288 s.
5. Pentin YU. A., Vilkov L. V. Fizychni metody doslidzhennya v khimiyi. - Moskva: Myr, TOV «Vydavnytstvo AST», 2003. - 683 s.
6. Inorganic Mass Spectrometry (Fundamentals and Applications) -Edited by Christopher M. Barshick, Douglas C. Duckworth, David H. Smith (Oak Ridge National Laboratory Oak Ridge, Tennessee) Marcel Dekker, Inc. New York • Basel – 2000. – 512 p.
7. High Performance Chelation Ion Chromatography / Pavel N. Nesterenko, Phil Jones, Brett Pauli – RSC Chromatography Monographs No. 14 - The Royal Society of Chemistry, 2011.– 303 p.
8. Ion Chromatography / James S. Fritz and Douglas T. Gjerde – Fourth edition. - WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim – 2009. –377 p.
9. Mass Spectrometry of Inorganic, Coordination and Organometallic Compounds: Tools - Techniques – Tips / William Henderson, J. Scott McIndoe. –John Wiley & Sons Ltd, 2005.- 271 p.
10. Handbook of Soil Analysis Mineralogical, Organic and Inorganic Methods / Marc Pansu, Jacques Gautheyrou - Springer Berlin Heidelberg New York, 2006. – 993 p.
2. Minayeva V. O. Khromatohrafichniy analiz. - Cherkasy: Vyd. vid. CHNU imeni Bohdana Khmel?nyts?koho, 2013. - 284 s.
3. Minaeva V.O. Metody kontsentruvannya neorhanichnikh Rechovyny / V.O. Minaeva. Navch-met. posibnyk. - Cherkasy: Vyd. vid. CHNU imeni Bohdana Khmel?nyts?koho, 2014. - 313 s.
4. Otto M. Suchasni metody analitychnoyi khimiyi (v 2-kh tomakh) Tom 2. Moskva: Tekhnosfera, 2004. – 288 s.
5. Pentin YU. A., Vilkov L. V. Fizychni metody doslidzhennya v khimiyi. - Moskva: Myr, TOV «Vydavnytstvo AST», 2003. - 683 s.
6. Inorganic Mass Spectrometry (Fundamentals and Applications) -Edited by Christopher M. Barshick, Douglas C. Duckworth, David H. Smith (Oak Ridge National Laboratory Oak Ridge, Tennessee) Marcel Dekker, Inc. New York • Basel – 2000. – 512 p.
7. High Performance Chelation Ion Chromatography / Pavel N. Nesterenko, Phil Jones, Brett Pauli – RSC Chromatography Monographs No. 14 - The Royal Society of Chemistry, 2011.– 303 p.
8. Ion Chromatography / James S. Fritz and Douglas T. Gjerde – Fourth edition. - WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim – 2009. –377 p.
9. Mass Spectrometry of Inorganic, Coordination and Organometallic Compounds: Tools - Techniques – Tips / William Henderson, J. Scott McIndoe. –John Wiley & Sons Ltd, 2005.- 271 p.
10. Handbook of Soil Analysis Mineralogical, Organic and Inorganic Methods / Marc Pansu, Jacques Gautheyrou - Springer Berlin Heidelberg New York, 2006. – 993 p.
Методи і критерії оцінювання:
Examination (written part 60% and oral component 40%).